九十七學年第二學期「化學實驗二」課程綱要
一、課程編號：203-11510-01, 02
二、教科書：
國立台灣大學化學系，「化學實驗一暨化學實驗二」，第二版，國立台灣大學出版中心，台北，2006.
教學網頁：http://www.ch.ntu.edu.tw/~genchem99/index.htm
https://ceiba.ntu.edu.tw/921edtech
三、成績評量方式：
實驗精神（態度）：40％ 預習報告：10％ 實驗紀錄：10%
實驗結果報告：20％ 實驗期末考：20％
四、預修課程：先修或併修「普通化學甲上下」。
五、課程進度：
第二學期
|
週 |
實驗名稱 |
配合普化課程內容 |
|
1 |
C0 報到分組、安全簡介 |
|
|
2 |
C14 高錳酸鉀的氧化還原滴定 |
氧還反應 |
|
3 |
C16 分光光譜法之應用－微量鈷離子定量 |
錯離子、光譜化學 |
|
4 |
C17 高溫超導體之製備 |
氧高溫超導體、固態反應法 |
|
5 |
C20 從廢鋁罐製備明礬 |
兩性化合物、錯合物及結晶 |
|
6 |
C21-1 碘鐘實驗－反應級數及活化能之測定 |
初期反應速率法 |
|
7 |
C21-2~4 碘鐘實驗－反應級數及活化能之測定 |
積分作圖法、活化能與催化劑 |
|
8 |
C22 溫度計之校正及可溶性物質分子量之測定 |
依數性質、凝固點下降 |
|
9 |
C_N 太陽能電池之製備 |
氧化還原反應、奈米材料、綠色化學 |
|
10 |
C23 蒸餾 |
有機化學 |
|
11 |
C24 分餾 |
有機化學 |
|
12 |
C25 萃取及有機酸在水與有機溶劑間之分佈 |
酸鹼、滴定、有機 |
|
13 |
C26 再結晶與熔點測定 |
溶液、共熔點 |
|
14 |
C27 層析法 |
薄層及管柱層析 |
|
|
期末考 |
97年6月13日星期五中午12:20-13:10 |
參考書：Harris, D. C. Quantitative Chemical Analysis, 5th ed., 1999, W. H. Freeman and Co.: New York.
Chemistry Lab. (II) (2008, Spring)
Textbook:
Department of Chemistry, National Taiwan University, Chemistry Laboratory (I), (II), 2nd ed., Taipei, 2006.
Website: http://www.ch.ntu.edu.tw/~genchem99/index.htm
https://ceiba.ntu.edu.tw/921edtech
Objective:
Chemistry Laboratory (I) and (II) are Integrated Laboratory courses to fulfill the requirements of Chemistry-majored students. The objectives are to demonstrate the principles of chemistry, teach the students various techniques used by chemists, and train the students to familiar with scientific methods.
Course descriptions:
The contents of Chemistry Laboratory (I) and (II) includes: stoichiometry, thermochemistry, acid-base, equilibrium, buffer solution, titration, electrochemistry, chemical kinetics, coordination compounds, spectrophotometry, materials science, and basic organic chemistry skills.
Course requirements:
Review the experiment before class. Follow the safety guidelines of Lab. Be familiar with Lab skills. Hand in reports on time. Attend the final exam at the end of semester.
Grading: Attitude: 40%; Report: 40%; Final exam: 20%
Contents: Chemistry (II)
|
1 |
Laboratory safety and work instructions |
|
2 |
C14. Oxidation/reduction titrations with potassium permanganate |
|
3 |
C_N Solar energy |
|
4 |
C16. Spectrophotometric analysis of cobaltous ions |
|
5 |
C17. Synthesis of Y-Ba-Cu superconductor |
|
6 |
C20. Preparation of alum from aluminum can |
|
7,8 |
C21. Iodine clock - the study of chemical kinetics (I), (II) |
|
9 |
C22. Molecular weight determination by freezing point depression |
|
10 |
C23. Simple distillation |
|
11 |
C24. Fractional distillation |
|
12 |
C25. Extraction |
|
13 |
C26. Recrystallization and melting point determination |
|
14 |
C27. Chromatography |